Electrochemical behaviour of a new percursor for the design of Poly[Ni(saltMe)]...

• Author(s): Vilas-Boas, Miguel ; Santos, I.C. ; Henderson, M.J. ; Freire, C. ; Hillman, A.R. ; Vieil, E.
• Date: 2003
• Persistent ID: http://hdl.handle.net/10198/5887
• Origin: Biblioteca Digital do IPB
• Subject(s): Modified electrodes; Salen
• Document Type: Article
• Language: English

Description

Wedescribe the potentiodynamic preparation and subsequent characterization of poly[Ni(3-MeOsaltMe)] films (surface concentration, 3 < ¡/nmol cm-2 < 350) in acetonitrile media. Coulometric and gravimetric (electrochemical quartz crystal microbalance, EQCM) data allow one to monitor the deposition process and show that the resultant films are physically and chemically stable.