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Electrochemical behaviour of a new percursor for the design of Poly[Ni(saltMe)]...
Vilas-Boas, Miguel; Santos, I.C.; Henderson, M.J.; Freire, C.; Hillman, A.R.; Vieil, E.Wedescribe the potentiodynamic preparation and subsequent characterization of poly[Ni(3-MeOsaltMe)] films (surface concentration, 3 < ¡/nmol cm-2 < 350) in acetonitrile media. Coulometric and gravimetric (electrochemical quartz crystal microbalance, EQCM) data allow one to monitor the deposition process and show that the resultant films are physically and chemically stable.
Data: 2003
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Origem: Biblioteca Digital do IPB
A combined electrochemical quartz-crystal microbalance probe beam deflection (E...
Vilas-Boas, Miguel; Henderson, M.J.; Freire, C.; Hillman, A.R.; Vieil, E.The oxidative polymerization of the complex2,3-dimelhyl-N,N-bis( salicylidene)butane-2,3-diaminatonickel( n), [Ni(saltMe)], was monitored by the electrochemical quartz microbalance (EQCM) and crystal impedance techniques. Polymerisation efficiency was maintained throughout deposition of a film, which behaved rigidly, on the electrode.
Data: 2000
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Origem: Biblioteca Digital do IPB
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