A flow injection system with in-line ion exchange is proposed for the spectrophotometric determination of lead in Port wine. A Chelex-100 resin mini-column (200–400 mesh) is used for lead concentration, and the chromogenic reaction is based on the formation of a ternary complex between lead, Malachite Green and iodide. Forty-five digested wine samples can be run per hour (25–500 µg l–1 Pb) and results are compa...
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