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SbCl5—wet acetonitrile: a new system for chemoselective O-desilylation
Glória, Paulo M. C.; Prabhakar, Sundaresan; Lobo, Ana M.; Gomes, MárioAbstract—A new efficient method for deprotection of TBDMS derivatives of phenols, primary alcohols, carboxylic acids and secondary amines, consisting of SbCl5 and MeCN with 0.1% water (w/v), is reported. It effects inter alia desilylation of a CH2OTBDMS group in the presence of a ketal function.
Data: 2003
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Origem: Repositório Científico do Instituto Politécnico de Lisboa
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