A method for determination of ochratoxin A (OTA) in wine grapes is described, using extraction with a hydrogen carbonate and polyethylene glycol (PEG) solution (5% NaHCO3 and 1% PEG 8000), followed by immunoaffinity clean-up and liquid chromatography with fluorescence detection. Validation was made with spiked samples, in levels of 0.05 and 1µg kg−1, with average recovery rates of 76% and relative standard devi...
Financiadores do RCAAP | |||||||
![]() |
![]() |
![]() |
![]() |
![]() |
![]() |