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Assumir o papel de pai: intervenção psicoterapêutica na adolescência

Identification and Preservation of Parathyroid Glands in Cadaver Parts

Introdução: É indispensável ter um conhecimento profundo da morfologia da glândula tiróide e das estruturas com ela relacionadas no compartimento anterior do pescoço, para minimizar a morbilidade decorrente da cirurgia da tiróide, nomeadamente a lesão das glândulas paratiróides e dos nervos laríngeos. Este estudo pretendeu identificar glândulas paratiróides em peças de cadáver, confirmando-as histologicamente.M...

The Anatomical Variations of the Extensor Muscles of the Hand Fingers

Introduction: The extensor tendons of fingers are subject of many variations, some of them quite frequent.Material and Methods: The dissection of the posterior region of forearm and hand was carried out, and the anatomical variations were documented.Results: In Case 1 the extensor digitorum divided into 5 tendons: one for the index finger, one for the middle finger, two for the ring finger and one for the littl...

Rare Anatomical Variation of Absence of the Sciatic Nerve: Completely Substitut...

Introduction: There are several reports of sciatic nerve anatomical variations. Some are associated with clinical entities, such as piriformis syndrome. We aim to report a rare anatomical variation of this nerve.Cases report: Two leucodermic, 74 and 78-year-old male subjects, deceased of natural causes, without lower limb relevant medical history. In both subjects, the right sciatic nerve was absent, with an in...

Ammonium ionic liquids as green solvents for drugs 

A high solubility of antituberculosis antibiotic drugs: isoniazid and pyrazinecarboxamide in ammonium ionic liquids shown in this work, demonstrates the promising perspectives in the drug processing. Solid–liquid equilibrium (SLE) measurements have been made using a dynamic (synthetic) method. Thermophyscial properties such as melting point, enthalpy of fusion, temperatures of phase transitions and correspondi...

Solubility of pharmaceutical compounds in ionic liquids

The solubility of N-acetyl-l-cysteine, coumarin and 4-hydroxycoumarin in alternative solvents was studied in this work. The solid–liquid equilibrium (SLE) measurements have been performed using a dynamic(synthetic) method. Melting points and enthalpies of fusion of the pharmaceutical compounds were acquired using a differential scanning calorimetry (DSC). The solubility of N-acetyl-l-cysteine and 4-hydroxycoum...

Supported metal catalysts for free fatty acid rich residues

A favourable solubility of isoniazid, an antitubercular antibiotic drug, in alt...

The sufficient solubility of isoniazid in alternative solvents obtained in this work can open new perspectives in pharmaceutical processing. Solid–liquid equilibrium (SLE) measurements have been made using a dynamic (synthetic) method. The melting point and the enthalpy of fusion of isoniazid were acquired using differential scanning calorimetry (DSC). The solubility of isoniazid in bis(trifluoromethylsulfonyl)...

Combination of supercritical carbon dioxide and ionic liquid in a novel assembl...

Exploitation of neoteric solvents in the efficient total synthesis of carvacrol, an antimicrobial reagent, has been accomplished. The first reaction aimed supercritical mediated heterogeneous hydrogenation of carvone catalysed by palladium. The second step guided to an application of great salvation capacity of ionic liquids in separation of carvacrol from the post-hydrogenation mixture. The process has been co...

Alternative solvents in carvone hydrogenation

Dissertação para obtenção do Grau de Mestre em Engenharia Química e Bioquimica ; Hydrogenation of monoterpenes, such as carvone, in high-density carbon dioxide over 0.5 wt.% Pd, or Rh, or Ru supported on alumina was investigated. Hydrogenation is generally faster in a single supercritical (sc) phase than in a biphasic system. The reaction catalysed by Pd produces full hydrogenated products (isomers of carvomen...