http://www.sciencedirect.com/science/article/B6TXM-4TRM3MB-3/2/a3801608d0695335d1eccf6692a4287d
A coarse-grained tetragonal sigma phase [sigma]-Fe0.54Cr0.46, prepared from an as-cast alloy, and a nanocrystalline [sigma]-Fe0.52Cr0.48 phase were ball-milled in argon in a Fritsch P0 ball-mill at different vibration amplitudes. X-ray diffraction evidences solely a gradual transformation of the sigma phases into bcc phases. Room-temperature Mössbauer spectroscopy shows further the presence of a non-magnetic ph...
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