Author(s):
Trindade, Tito 
; O' Brien, Paul ; Zhang, Xiao-mei ; Motevallii, Majid
Date: 1997
Persistent ID: http://hdl.handle.net/10773/5776
Origin: RIA - Repositório Institucional da Universidade de Aveiro
Document details
Synthesis of PbS nanocrystallites using a novel single molecule precursors appr...
Description
The synthesis and characterisation of some lead(II) dithiocarbamato complexes Pb(S2CNRR¾)2 is reported. These compounds were used as single molecule precursors to produce nanocrystalline PbS by their thermolysis in trioctylphosphine oxide. The optical and morphological properties of the resulting PbS nanocrystallites were investigated; the influence of experimental parameters, such as precursor, growth time and temperature, on the final nanodispersed materials is also reported.
The synthesis and characterisation of some lead(II) dithiocarbamato complexes Pb(S2CNRR¾)2 is reported. These compounds were used as single molecule precursors to produce nanocrystalline PbS by their thermolysis in trioctylphosphine oxide. The optical and morphological properties of the resulting PbS nanocrystallites were investigated; the influence of experimental parameters, such as precursor, growth time and temperature, on the final nanodispersed materials is also reported.
Document Type
Article
Language English
Language English
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