Thermal and structural analysis of 4,5,6-trimethoxyisatin

• Autor(es): Campos, Ana M. F. Oliveira ; Rodrigues, Lígia M. ; Francisco, Carla Santana ; Oliveira, M. J. ; Silva, Maria Manuela ; Smith, Michael John ; Paz, Filipe A. Almeida
• Data: 2009
• Identificador Persistente: http://hdl.handle.net/1822/10484
• Origem: RepositóriUM - Universidade do Minho
• Assunto(s): Isatin; DSC; TGA; Hot-stage microscopy; Single-crystal X-ray diffraction (XRD)
• Tipo de Documento: Artigo
• Idioma: Inglês

Descrição

4,5,6-Trimethoxyisatin was crystallized from water to give dark red needles that were characterized by NMR and IR spectroscopy, differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), single-crystal X-ray diffraction (XRD) and hot-stage microscopy.